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The energy-free purification of trace thallium(I)-contaminated potable water using a high-selective filter

《化学科学与工程前沿（英文）》 doi: 10.1007/s11705-023-2379-8

摘要： Thallium is a highly toxic metal, and trace amount of thallium(I) (Tl+) in potable water could cause a severe water crisis, which arouses the exploitation of highly-effective technology for purification of Tl+ contaminated water. This report proposes the multi-layered Prussian blue (PB)-decorated composite membranes (PBx@PDA/PEI-FP) based on the aminated filter papers for Tl+ uptake. Extensively characterization by Fourier transform infrared spectrometer-attenuated total reflectance, scanning electron microscope, thermogravimetric analysis, X-ray photoelectron spectroscopy and X-ray diffraction were performed to confirm the in situ growth of cubic PB crystals on filter paper membrane surfaces via the aminated layers, and the successful fabrication of multi-layered PB overcoats via the increasing of aminated layers. The effect of PB layers on Tl+ removal by PBx@PDA/PEI-FP from simulated drinking water was evaluated as well as the influence of different experimental conditions. A trade-off between PB decoration layer number and PB distribution sizes is existed in Tl+ uptake by PBx@PDA/PEI-FP. The double-layered PB2@PDA/PEI-FP membrane showed the maximum sorption capacity, but its Tl+ uptake performance was weakened by the acid, coexisting ions (K+ and Na+) and powerful operation pressure, during filtrating a large volume of low-concentrated Tl+-containing water. However, the negative effect of coexisting ions on the Tl+ uptake could be effectively eliminated in weak alkaline water, and the Tl+ removal was increased up to 100% without any pressure driving for PB2@PDA/PEI-FP membrane. Most importantly, PB2@PDA/PEI-FP displayed the high-efficiency and high-selectivity in purifying the Tl+-spiked Pearl River water, in which the residual Tl+ in filtrate was less than 2 μg·L–1 to meet the drinking water standard of United States Environmental Protection Agency. This work provides a feasible avenue to safeguard the drinking water in remote and underdeveloped area via the energy-free operation.

关键词： membrane adsorption     Prussian blue     energy-free filtration     potable water     trace thallium(I)    

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removal of heavy metals from industrial wastewater: Bench and pilot scale studies focusing on in-depth thallium

Huosheng Li, Hongguo Zhang, Jianyou Long, Ping Zhang, Yongheng Chen

《环境科学与工程前沿（英文）》 2019年 第13卷 第4期 doi: 10.1007/s11783-019-1130-7

摘要：

Addition of alkali to pH 10 is effective for precipitation of precipitable metals.

Fenton treatment is effective for substantial removal of Tl, Cd, Cu, Pb, and Zn.

Sulfide precipitation is a final step for removal of trace Tl, Cd, Cu, Pb, and Zn.

Bench and pilot studies demonstrated the effectiveness of this combined technique.

关键词： Thallium     Pilot     Fenton     Sulfide precipitation     Heavy metal     Industrial wastewater    

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Zero-valent manganese nanoparticles coupled with different strong oxidants for thallium removal from

Keke Li, Huosheng Li, Tangfu Xiao, Gaosheng Zhang, Aiping Liang, Ping Zhang, Lianhua Lin, Zexin Chen, Xinyu Cao, Jianyou Long

《环境科学与工程前沿（英文）》 2020年 第14卷 第2期 doi: 10.1007/s11783-019-1213-5

摘要： • Nano zero-valent manganese (nZVMn, Mn0) is synthesized via borohydrides reduction. • Mn0 combined with persulfate/hypochlorite is effective for Tl removal at pH 6-12. • Mn0 can activate persulfate to form hydroxyl and sulfate radicals. • Oxidation-induced precipitation and surface complexation contribute to Tl removal. • Combined Mn0-oxidants process is promising in the environmental field. Nano zero-valent manganese (nZVMn, Mn0) was prepared through a borohydride reduction method and coupled with different oxidants (persulfate (S2O82−), hypochlorite (ClO−), or hydrogen peroxide (H2O2)) to remove thallium (Tl) from wastewater. The surface of Mn0 was readily oxidized to form a core-shell composite (MnOx@Mn0), which consists of Mn0 as the inner core and MnOx (MnO, Mn2O3, and Mn3O4) as the outer layer. When Mn0 was added alone, effective Tl(I) removal was achieved at high pH levels (>12). The Mn0-H2O2 system was only effective in Tl(I) removal at high pH (>12), while the Mn0-S2O82− or Mn0-ClO− system had excellent Tl(I) removal (>96%) over a broad pH range (4–12). The Mn0-S2O82− oxidation system provided the best resistance to interference from an external organic matrix. The isotherm of Tl(I) removal through the Mn0-S2O82− system followed the Freundlich model. The Mn0 nanomaterials can activate persulfate to produce sulfate radicals and hydroxyl radicals. Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy suggested that oxidation-induced precipitation, surface adsorption, and electrostatic attraction are the main mechanisms for Tl(I) removal resulting from the combination of Mn0 and oxidants. Mn0 coupled with S2O82−/ClO− is a novel and effective technique for Tl(I) removal, and its application in other fields is worthy of further investigation.

关键词： Nano zero-valent manganese     Thallium     Adsorption     Oxidation     Sulfate radical     Hydroxyl radical    

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Assessment of mobile and potential mobile trace elements extractability in calcareous soils using different

Mohsen Jalali, Ziba Hurseresht

《环境科学与工程前沿（英文）》 2020年 第14卷 第1期 doi: 10.1007/s11783-019-1186-4

摘要： DTPA and NH4OAc, HNO3 and EDTA, and MgCl2 and NH4NO3 had similar behavior. In NH4OAc, DTPA, and EDTA, the possibility of re-adsorption of trace elements is low. CaCl2 may be more suitable than other extracts in calcareous soils. Understanding trace elements mobility in soils, extracting agents, and their relationships with soil components, are essential for predicting their movement in soil profile and availability to plants. A laboratory study was conducted to evaluate extractability of cadmium (Cd), cobalt (Co), copper (Cu), nickel (Ni), and zinc (Zn) from calcareous soils utilizing various extracting agents to be specific CaCl2, DTPA, EDTA, HNO3, MgCl2, NaNO3, NH4NO3, and NH4OAc. Cluster analysis indicated that DTPA and NH4OAc, HNO3 and EDTA, and MgCl2 and NH4NO3 extracting agents yielded comparative values, whereas NaNO3 and CaCl2 have shown different behavior than other extracting agents for all studied trace elements. The speciation of extracted trace elements in solutions indicated that in the CaCl2, NaNO3, NH4NO3, and MgCl2 extracting agents most extracted Cd, Co, Ni, Zn, and part of Cu were as free ions and may be re-adsorbed on soils, leading to lower extractability, whereas, in the case of HNO3 extracting agent, the likelihood of re-adsorption of trace elements may be little. The results of speciation of trace elements using NH4OAc, DTPA, and EDTA extracting agents showed that Me-(Acetate)3–, Me-(Acetate)2(aq), Me(DTPA)3−, Me(EDTA)2−, and MeH(EDTA)– complexes dominated in solutions indicating that the extracted trace elements may not be re-adsorbed on soils, leading to higher extractability. The results of this study are useful for short and long-term evaluations of trace elements mobility and further environmental impacts.

关键词： Mobility     Calcareous soils     Extracting agents     Trace elements    

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Preconcentration of trace elements by adsorption onto a niobium wire for electrothermal atomization atomic

Satoshi KANECO, Hiroaki KITANAGA, Hideyuki KATSUMATA, Tohru SUZUKI

《化学科学与工程前沿（英文）》 2012年 第6卷 第4期   页码 432-435 doi: 10.1007/s11705-012-1219-z

摘要： In the present work, a new preconcentration method of trace elements by adsorption onto a niobium wire has been developed for electrothermal atomization atomic absorption spectrometry (ETAAS) with a tungsten tube atomizer. Detection limits (pg·mL ) by this method combined with ETAAS were 45 for bismuth, 7.0 for cadmium, 20 for copper, 1.3 for gold, 36 for lead, 65 for manganese, 9.5 for rhodium and 19 for silver.

关键词： preconcentration     adsorption onto niobium wire     electrothermal atomization atomic absorption spectrometry     tungsten tube atomizer     trace elements    

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Assessing human bioaccessibility of trace contaminants in size-fractionated red mud, derived precipitates

Chunfeng Wang, Yanchen Zhu, Dan Yao, Guanfei Chen, Lianjun Wang

《环境科学与工程前沿（英文）》 2017年 第11卷 第6期 doi: 10.1007/s11783-017-0956-0

摘要： The objective of this study was to provide insight into human exposure to trace contaminants bearing red mud, derived precipitates and geopolymeric blocks due to inhalation contact and/or hand-to-mouth ingestion. The in vitro bioaccessibility behavior of trace contaminants was investigated with the PBET (physiologically based extraction test), ALF (artificial lysosomal fluid) and MGS (modified Gamble’ solution) methods. The results showed that total contents of trace contaminants and operation parameters, such as pH and chelating properties of simulated gastrointestinal phases (PBET), played a joint role in controlling the bioaccessibility efficacy for size-fractionated red mud particles. As for airborne particles (<38 µm size fractions), trace contaminants concentrations extracted by MGS was significantly higher than those by ALF. Additionally, higher bioaccessibility (PBET) values of Cu, Pb, Zn, As, V and U were obtained from red mud derived precipitates compared with those of red mud itself. Even though short-term and long-term leaching values of trace contaminants were relatively lower in the prepared geopolymeric blocks, the health risk could be significantly higher due to the more pronounced bioaccessibility characteristics.

关键词： Bioaccessibility     Trace contaminants     Red mud     Precipitates     Geopolymeric blocks.    

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Biodegradation of trace pharmaceutical substances in wastewater by a membrane bioreactor

Longli BO, Taro URASE, Xiaochang WANG

《环境科学与工程前沿（英文）》 2009年 第3卷 第2期   页码 236-240 doi: 10.1007/s11783-009-0004-9

摘要： The biodegradation of selected pharmaceutical micropollutants, including two pharmaceuticals with argued biodegradation, was studied by a lab-scale membrane bioreactor. The reaction kinetics and affecting factors were also investigated in this paper. Clofibric acid (CA) with contradictive biodegradation reported was degraded almost completely at different hydraulic retention times (HRTs) after adaptation to microorganisms. The biodegradation of CA was disturbed at low pH operation, while the activity of microorganisms recovered again after pH adjustment to neutral condition. Ibuprofen (IBP) degraded under neutral and acidic conditions. Removals of IBP and CA were zero-order and first-order reactions under high and low initial concentrations, respectively. Carbamazepine and diclofenac were not degraded regardless of HRTs and pH.

关键词： pharmaceuticals     membrane bioreactor     activated sludge     reaction kinetics    

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PSS sorbents for removing trace hydrogen sulfide in methane

Limei ZHONG, Li ZHOU

《化学科学与工程前沿（英文）》 2011年 第5卷 第3期   页码 339-342 doi: 10.1007/s11705-010-0569-7

摘要： Sorbents of the pressure swing sorption process (PSS) to remove trace amount of H S (190 ppm) contained in methane were experimentally studied. The sorbents consist of adsorbent carrier (silica gel or activated carbon) and absorbent which spreads outside the carrier granules’ pores (triethanolamine, TEA or -methyl-2-pyrrolidone, NMP). The results of breakthrough and regeneration tests show that silica gel is more suitable to be the carrier than activated carbon and TEA is more suitable to be the absorbent than NMP. The loaded absorbent could enlarge the sorption capacity of H S considerably. And the BET tests indicate that the absorbent deposits on the surface of the carrier’s pores and can reduce the mesopores’ size and block the micropores.

关键词： pressure swing sorption     H2S     methane     carrier     absorbent    

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Error compensation for tool-tip trace during cutting of laminated paper for rapid prototyping

Yucheng DING, Changhe LI, Dichen LI, Guoxin YU

《机械工程前沿（英文）》 2009年 第4卷 第2期   页码 111-119 doi: 10.1007/s11465-009-0020-2

摘要： Laminated object manufacturing (LOM) is one of the commercialized rapid prototyping (RP) processes, where a focused laser is usually used to cut the cross-section contours of a 3 D part and the grid hatchings of the part-exterior region on a sheet paper stack-wise. Using a laser beam as a cutter can be costly, and the thermal burning of a sheet paper along a laser scanning path can also cause an environment-polluting smoke. This paper presents a paper laminating RP system using a knife as the paper cutter instead of a laser beam. The knife holder is mounted through a radial bearing on the - positioning mechanism in such a way that the knife tip is eccentric to the bearing axis by a small distance (so-called offset). Therefore, the knife tip, which engages into the sheet paper during cutting, tends to follow the path of the -driven bearing axis by the error that depends on the path tangential and the eccentricity of the knife tip. A tractrix model is applied to describe the kinetic motion of the knife tip and a method is formulated to compensate for the tracing error of the eccentric knife tip by modifying the original cross-section contours of the part for each layer based on the tractrix equation. A study has also been performed regarding the effect of the knife tip geometry on the cutting notch of the sheet paper and on the roughness of the finished part.

关键词： rapid prototyping     laminated object manufacturing     knife-cutting     tracing error    

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Occurrence and health risk assessment of trace heavy metals via groundwater in Shizhuyuan Polymetallic

Bingbing XU,Qiujin XU,Cunzhen LIANG,Li LI,Lijia JIANG

《环境科学与工程前沿（英文）》 2015年 第9卷 第3期   页码 482-493 doi: 10.1007/s11783-014-0675-8

摘要： The Shizhuyuan Polymetallic Mine in Chen-zhou City is an important multi-metal deposit in China. After a dam accident in 1985, there are still a number of mining plants, smelters and tailing ponds in this area. These had the potential to pollute the surrounding groundwater. In this study, groundwater samples were collected from 20 residents’ wells in this area during both dry and wet seasons. In particular, this study focused on the exposure and the health risk assessment of trace heavy metal in groundwater. Multiple statistical analysis and fuzzy comprehensive method were employed to reveal the distribution characteristics of heavy metal and to assess the groundwater quality. Results indicated that Cr, Fe, Ni, Cu, Zn, As, Cd, Ba, Hg and Pb were widespread with low exposure levels. There were 19 wells with low level exposure and one well with a moderate level exposure in the dry season. All of the wells were in low level exposure during the wet season. As and Mn exhibited potential non-carcinogenic concern, because their maximum hazard quotient (HQ) was higher than 1.0. This may cause adverse health effect on adults in dry season or on children in both seasons. Only As, showed that the maximum carcinogenic risk was more than 10 , suggesting a high cancer risk for children in both dry and wet seasons. Therefore, analysis and reduction the concentrations of As and Mn in groundwater are needed in order to protect the health of residents and especially children in the area.

关键词： groundwater     heavy metal     health risk assessment     mine area    

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Research progress in removal of trace carbon dioxide from closed spaces

ZHANG Yatao, FAN Lihai, ZHANG Lin, CHEN Huanlin

《化学科学与工程前沿（英文）》 2007年 第1卷 第3期   页码 310-316 doi: 10.1007/s11705-007-0057-x

摘要： In this paper, the removal of trace carbon dioxide from closed spaces through membrane process and biotransformation are introduced in detail. These methods include the microalgae photobioreactor, membrane microalgae photobioreactor, supported liquid membrane, membrane gas-liquid contactor, hydrogel membrane, and enzyme membrane bioreactor. The advantages and disadvantages of these methods are compared. It is found that higher CO removal efficiency can be obtained in biotransformation and membrane process. However, a large volume and high energy consumption are needed in biotransformation, while the low permeability and stability must be solved in the membrane process.

关键词： removal efficiency     consumption     removal     CO removal     membrane microalgae    

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Degradation of trace nitrobenzene in water by microwave-enhanced H

Honghu ZENG, Lanjing LU, Meina LIANG, Jie LIU, Yanghong LI

《环境科学与工程前沿（英文）》 2012年 第6卷 第4期   页码 477-483 doi: 10.1007/s11783-012-0395-x

摘要： To evaluate possible use of microwave-enhanced H O -based (MW/H O ) process to degrade trace nitrobenzene (NB) in water, a series of batch experiments were conducted. The results showed that 2450MHz microwave irradiation significantly enhanced oxidative decomposition of nitrobenzene (NB) in a H O system. About 90% NB was degraded by the MW/ H O process in 30 min. Moreover, the MW/ H O process could enhanced the oxidative degradation of NB even at relatively low temperature (50°C). When the initial concentration of NB was 300μg/L, the optimum ratio of H O to NB and MW power were 70 and 300 W respectively. The presence of humic acid significantly increased H O dosage. The ultraviolet absorbance at 254 nm (UV ) indicated degradation of NB was stepwise and some intermediates were produced. The gas chromatography-mass spectrometric (GC-MS) analysis showed that main intermediates were nitrophenolic and carbonyl compounds.

关键词： microwave     hydrogen peroxide     nitrobenzene     humic acid    

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Preliminary study of trace element emissions and control during coal combustion

ZHANG Junying, ZHAO Yongchun, DING Feng, ZENG Hancai, ZHENG Chuguang

《能源前沿（英文）》 2007年 第1卷 第3期   页码 273-279 doi: 10.1007/s11708-007-0038-2

摘要： Hazardous trace element emissions have caused serious harm to human health in China. Several typical high-toxic trace element coals were collected from different districts and were used to investigate the emission characteristics of toxic trace elements (As, Se, Cr, Hg) and to explore preliminary control methods. Coal combustion tests were conducted in several bench-scale furnaces including drop tube furnace (DTF), circulating fluidized bed (CFB) combustion furnace, and fixed-bed combustion furnace. Calcium oxide was used to control the emission of arsenic and selenium. The granular activated carbons (AC) and activated-carbon fibers (ACF) were used to remove mercury in the flue gas from coal combustion. The chemical composition and trace element contents of ash and particulate matter (PM) were determined by X-ray fluorescence (XRF) spectrometry and inductively coupled plasma-atomic emission spectrometry (ICP-AES), respectively. The speciation and concentration of mercury were investigated using the Ontario-Hydro method. X-ray diffraction spectrometry (XRD) was used to determine the mineral composition of production during combustion experiments. With the addition of a calcium-based sorbent, arsenic concentration in PM sharply decreased from 0.25–0.11 mg/m. In fixed-bed combustion of coal, the retention rates of selenium volatiles were between 11.6% and 50.7% using lime. In the circulating fluidized-bed combustion of coal, the content of selenium in ash from the chimney was reduced to one-fourth of its original value and that in leaching water from the chimney decreased by two orders of magnitude using lime. Calcium-based sorbent is an effective additive to control the emission of As and Se during coal combustion. The emission of chromium is influenced by the occurrence mode of Cr in coal. Chromium emission in PM during coal combustion is 55.5 and 34.7 μg/m for Shenbei coal and mixed Pingdingshan coal, respectively. The adsorptive capacity of granular activated carbon for Hg is significantly enhanced through ZnCl-impregnation. The activated carbon fibers showed decent efficiency in mercury adsorption, on which surface oxygen complex showed positive effects on mercury adsorption.

关键词： Pingdingshan     occurrence     plasma-atomic emission     chemical composition     Several typical    

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Feasibility study on simultaneous removal of sulfur and trace selenium in the MTD-FGD reactor

LI Yuzhong, TONG Huiling, ZHUO Yuqun, LI Yan, CHEN Changhe, XU Xuchang

《能源前沿（英文）》 2007年 第1卷 第3期   页码 259-263 doi: 10.1007/s11708-007-0036-4

摘要： This study deals with the simultaneous removal of sulfur dioxide (SO) and trace selenium dioxide (SeO) from flue gas by calcium oxide (CaO) adsorption in the moderate temperature range, especially the feasibility of simultaneous removal of these two pollutants in a moderate temperature dry flue gas desulfurization (MTD-FGD) reactor. The effect of SO presence on selenium capture is studied through the experiments performed on a thermogravimetric analyzer (TGA) and the following conclusions can be obtained. When CaO conversion is relatively low and the reaction rate is controlled by chemical reaction kinetics, the SO presence does not affect selenium capture. When CaO conversion is very high and the reaction rate is controlled by product layer diffusion, the SO presence and the product layer diffusion resistance jointly reduce selenium capture. Through analyses of some pilot scale MTD-FGD tests, it can be concluded that in the MTD-FGD reactor, the sulfate reaction of sorbent particles is generally kinetically controlled. Therefore, it is feasible that sulfur and trace selenium can be simultaneously removed by Ca-based sorbent in the MTD-FGD reactor.

关键词： Ca-based sorbent     product     feasibility     thermogravimetric analyzer     simultaneous removal    

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Ultrasound-assisted emulsification solidified floating organic drop microextraction for the determination of trace

Qingyun CHANG, Jingwen ZHANG, Xin DU, Jingjun MA, Jingci LI,

《环境科学与工程前沿（英文）》 2010年 第4卷 第2期   页码 187-195 doi: 10.1007/s11783-010-0030-7

摘要： A simple and efficient liquid-phase microextraction (LPME) technique was developed using ultrasound-assisted emulsification solidified floating organic drop microextraction (USAE-SFODME) combined with flame atomic absorption spectrometry, for the extraction and determination of trace copper in water samples. 1-(2-Pyridylazo)-2-naphthol (PAN) was used as chelating agent. Microextraction efficiency factors (including extraction solvent type, extraction volume, time, temperature, and pH), the amount of the chelating agent, and salt effect were investigated and optimized. Under the optimum extraction conditions, figures of merit of the proposed method were evaluated. The calibration graph was linear in the range of 20–600 g·L with a detection limit of 0.76 g·L. The relative standard deviation (R.S.D) for ten replicate measurements of 20 and 400 g·L of copper was 3.83% and 2.65%, respectively. Finally, the proposed method was applied to tap water, river water, and sea water, and accuracy was assessed through the analysis of certified reference water or recovery experiments.

关键词： ultrasound-assisted emulsification     solidified floating organic drop microextraction     flame atomic absorption spectrometry     preconcentration     copper    

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标题 作者 时间 类型 操作

The energy-free purification of trace thallium(I)-contaminated potable water using a high-selective filter

期刊论文

removal of heavy metals from industrial wastewater: Bench and pilot scale studies focusing on in-depth thallium

Huosheng Li, Hongguo Zhang, Jianyou Long, Ping Zhang, Yongheng Chen

期刊论文

Zero-valent manganese nanoparticles coupled with different strong oxidants for thallium removal from

Keke Li, Huosheng Li, Tangfu Xiao, Gaosheng Zhang, Aiping Liang, Ping Zhang, Lianhua Lin, Zexin Chen, Xinyu Cao, Jianyou Long

期刊论文

Assessment of mobile and potential mobile trace elements extractability in calcareous soils using different

Mohsen Jalali, Ziba Hurseresht

期刊论文

Preconcentration of trace elements by adsorption onto a niobium wire for electrothermal atomization atomic

Satoshi KANECO, Hiroaki KITANAGA, Hideyuki KATSUMATA, Tohru SUZUKI

期刊论文

Assessing human bioaccessibility of trace contaminants in size-fractionated red mud, derived precipitates

Chunfeng Wang, Yanchen Zhu, Dan Yao, Guanfei Chen, Lianjun Wang

期刊论文

Biodegradation of trace pharmaceutical substances in wastewater by a membrane bioreactor

Longli BO, Taro URASE, Xiaochang WANG

期刊论文

PSS sorbents for removing trace hydrogen sulfide in methane

Limei ZHONG, Li ZHOU

期刊论文

Error compensation for tool-tip trace during cutting of laminated paper for rapid prototyping

Yucheng DING, Changhe LI, Dichen LI, Guoxin YU

期刊论文

Occurrence and health risk assessment of trace heavy metals via groundwater in Shizhuyuan Polymetallic

Bingbing XU,Qiujin XU,Cunzhen LIANG,Li LI,Lijia JIANG

期刊论文

Research progress in removal of trace carbon dioxide from closed spaces

ZHANG Yatao, FAN Lihai, ZHANG Lin, CHEN Huanlin

期刊论文

Degradation of trace nitrobenzene in water by microwave-enhanced H

Honghu ZENG, Lanjing LU, Meina LIANG, Jie LIU, Yanghong LI

期刊论文

Preliminary study of trace element emissions and control during coal combustion

ZHANG Junying, ZHAO Yongchun, DING Feng, ZENG Hancai, ZHENG Chuguang

期刊论文

Feasibility study on simultaneous removal of sulfur and trace selenium in the MTD-FGD reactor

LI Yuzhong, TONG Huiling, ZHUO Yuqun, LI Yan, CHEN Changhe, XU Xuchang

期刊论文

Ultrasound-assisted emulsification solidified floating organic drop microextraction for the determination of trace

Qingyun CHANG, Jingwen ZHANG, Xin DU, Jingjun MA, Jingci LI,

期刊论文